Pseudoephedrine Acetate
Just a reprint. What do I think? Well, I would like the titled material to be analogous to chloroephedrine, but this is just a salt of the amine using acetic as the acid, a result of the isolation process from pills. Much of it is in traffic in Mexico; apparently the superlabs also purchase material which at one time was in pills. The second article is about a seizure.
Meth Synthesis W/ephedrine, HI, Red Phosphorus
by Cousin Singe
NOTICE: TO ALL CONCERNED Certain text files and messages contained on this site deal with activities and devices which would be in violation of various Federal, State, and local laws if actually carried out or constructed. The webmasters of this site do not advocate the breaking of any law. Our text files and message bases are for informational purposes only. We recommend that you contact your local law enforcement officials before undertaking any project based upon any information obtained from this or any other web site. We do not guarantee that any of the information contained on this system is correct, workable, or factual. We are not responsible for, nor do we assume any liability for, damages resulting from the use of any information on this site.
All you people who want an easy meth systhesis – They don’t exist! You have to know some chemistry. Learn some (yes it takes some discipline) or be doomed to fail.
So, again, this information is posted for information purposes only. I accept no responsibility for anyone actually using this. If you do you will be subject to state and federal laws and will be subject to fines and/or imprisonment. If you are stupid enough to actually manufacture meth you WILL probably go to prison. This is the 90's.
So to make meth from ephedrine- Using l- or pseudo ephedrine place 1000 gms of ephedrine, 250gms of red phosphorus, and 1000ml of hydriotic acid in a suitable round bottom flask. Fit the flask with a reflux condenser and reflux the mixture for 48hrs at 120 degrees C. Add a 10% solution of sodium hydroxide until the Ph is 14. You should get an oil layer and a water layer. Separate the oil layer in a separatory funnel and put it a flask with 3 volumes of water. Rig the flask for distillation and distill the oil water mixture until the oil is mostly gone (except for highly colored globs of oil.) In the reciever flask there should be two layers, an upper oil layer and a lower water layer. Separate the oil layer and mix it with 10% hydrochloric acid until the Ph is 7.6. evaporate the water and it will crystallize into methamphetamine hcl.
——
“We have observed that mixtures containing red phosphorus, iodine and either concentrated HCl or glacial acetic acid do convert ephedrine to methamphetamine; however, when the phosphorus is omitted, methamphetamine is not formed. Ephedrine was reacted with red phosphorus and iodine in refluxing water, varying the ratios of red phosphorus and iodine; when red phosphorus and iodine are in excess of ephedrine in a 1:3.8:7.2 molar ratio (ephedrine:red phosphorus:iodine) methamphetamine is formed and the ephedrine is consumed in 8 hours.”
Anyone have any thoughts, experience with the typical E-RP-HA when the usually separate step of creating the hydriotic acid is omitted and the three chemicals are just reacted in refluxing water. It seems like that is what is being described (along with acid substitution).
——
Materials:
1. 30ml bottle tincture iodine containing 2% iodine, sodium iodide 2.4%, alcohol 47%, rest H20
2. 5 Sinustop Herbal Decongestant tablets containing 60mg crystaline pseudoephedrine HCl each mixed with some herbal ingrediants. Or 300mg of ephedrine obtained thru some other method.
3. 5 road flares.
4. Bottle of drain cleaner containg conc. H2SO4
5. Bottle white distilled vinegar
6. Red devil Lye containing sodium hydroxide
7. Spray can of brake cleaner containing 1,1,1 trichloroethylene or 1,1,1 trichloroethane
Procedure:
A. Purifying pseudoephedrine:
1. Take the 5 decongestant capsules, empty their contents into a small funnel with a coffee filter. Pour 50ml of cold water through the filter, and collect the liquid in a small jar.
2. Add a 1/4tsp of lye to the collected liquid. You should immediately smell the odor of ephedrine.
3. Put the resultant solution in another small jar, and add 50ml of brake cleaner, then close the lid and shake vigorously. Let stand so that the layers seperate.
4. Using a turkey baster, suck up the bottom brake cleaner layer out of the jar and put it into a small bowl.
5. Add 50ml of vinegar and heat the resultant mixure over low heat in a frying pan with 1/2 inch of water. Thus a water bath. Do not use a gas stove, since the brake cleaner vapors will produce toxic phosgene if there is contact with a flame. Instead use a hot plate or electric stove at low heat only.
6. Heat the bowl in the water bath until no more liquid is left. At the bottom will be a solid layer of a pseudoephedrine acetate.
B. Preparing the red phosphorus:
1. Scrape the red phosphorus off of the caps of the 5 flares and store for later use. You should get about 0.1g per flare.
C. Preparing the iodine/HI solution:
1. Pour the entire bottle of the iodine tincture into a small ceramic bowl. Heat on the above type water bath until no more alcohol is left. Let cool, put in a small polyethylene jar, and add 0.1ml of the H2SO4 drain cleaner. Thats about 1/4inch of liquid in the end of an eye dropper. This converts the sodium iodide to HI. You now have a solution of iodine and HI. 2. Add the red phosphorus, and heat bottle in a water bath until the purple iodine color goes away.
D. The reaction:
1. Add the pseudoephedrine acetate to the solution of HI/I and phosphorus, and heat on a water bath for 24 hours.
E: Extraction:
1. Cool the reaction solution and add 1/2tsp of lye. Take the solution and perform steps A3-A6. 2. You will end up with methamphetamine acetate that you can scrape from the bowl.
Congradulations! You have circumvented all of law enforcement and have greatly contributed to the end of the “drug war”. (or contributed to the outlaw of all flares, iodine tincture, vignegar, drain cleaners, and auto store chemicals and coffee filters as will happen in the next year)
Best regards, Cousin Singe
————
FAQ fodder…
If methamphetamine looks waxy or oily, it is probably contaminated with the HI salt of meth, an oily by-product of the red-phosphorous/HI reduction of ephedrine–the most prevalent method of clandestine manufacture.
The HI salt is soluble in acetone, while the HCL salt is only very slightly soluble. The HI salt could be washed out, basified, and then precipitated with HCl gas to give methamphetmine HCL.
When completely dry, methamphetamine HCL is soluble in chloroform, while ephedrine HCL is not. This would provide a convenient method of separation.
[Reference: Skinner, Harry F., "Methamphetamine Synthesis Via Hydriotic Acid/Red Phosphorous Reduction Of Ephedrine," Forensic Science International, Vol 48, 1990, pp. 123-134]
Pseudoephedrine AcetateJust a reprint. What do I think? Well, I would like the titled material to be analogous to chloroephedrine, but this is just a salt of the amine using acetic as the acid, a result of the isolation process from pills. Much of it is in traffic in Mexico; apparently the superlabs also purchase material which at one time was in pills. The second article is about a seizure.Meth Synthesis W/ephedrine, HI, Red Phosphorusby Cousin SingeNOTICE: TO ALL CONCERNED Certain text files and messages contained on this site deal with activities and devices which would be in violation of various Federal, State, and local laws if actually carried out or constructed. The webmasters of this site do not advocate the breaking of any law. Our text files and message bases are for informational purposes only. We recommend that you contact your local law enforcement officials before undertaking any project based upon any information obtained from this or any other web site. We do not guarantee that any of the information contained on this system is correct, workable, or factual. We are not responsible for, nor do we assume any liability for, damages resulting from the use of any information on this site.All you people who want an easy meth systhesis – They don’t exist! You have to know some chemistry. Learn some (yes it takes some discipline) or be doomed to fail.So, again, this information is posted for information purposes only. I accept no responsibility for anyone actually using this. If you do you will be subject to state and federal laws and will be subject to fines and/or imprisonment. If you are stupid enough to actually manufacture meth you WILL probably go to prison. This is the 90's.So to make meth from ephedrine- Using l- or pseudo ephedrine place 1000 gms of ephedrine, 250gms of red phosphorus, and 1000ml of hydriotic acid in a suitable round bottom flask. Fit the flask with a reflux condenser and reflux the mixture for 48hrs at 120 degrees C. Add a 10% solution of sodium hydroxide until the Ph is 14. You should get an oil layer and a water layer. Separate the oil layer in a separatory funnel and put it a flask with 3 volumes of water. Rig the flask for distillation and distill the oil water mixture until the oil is mostly gone (except for highly colored globs of oil.) In the reciever flask there should be two layers, an upper oil layer and a lower water layer. Separate the oil layer and mix it with 10% hydrochloric acid until the Ph is 7.6. evaporate the water and it will crystallize into methamphetamine hcl.——"我々 は観察した赤いリン、ヨウ素と濃 HCl または氷酢酸を含有する混合物はエフェドリンを覚醒剤; に変換します。しかし、リンが省略されて、メタンフェタミンは形成されません。赤いリン、赤リンとヨウ素; の比率を変化させる水を還流でヨウ素と反応したエフェドリン赤リンとヨウ素が 1:3.8:7.2 のモル比 (エフェドリン: 赤リン: ヨウ素) 覚醒剤のエフェドリンを超えるが形成され、エフェドリンは 8 時間で消費される」。誰もが任意の考えは、hydriotic 酸を作成する通常別のステップを省略すると、3 つの化学物質の還流水に反応しているだけの典型的な E-RP-HA で経験あります。それは、(酸置換) と一緒に記載されているものであるように思えます。——材料:1. 30 ml ボトル チンキ ヨウ素アルコール 47%、ナトリウム ヨウ化 2.4% 2% ヨウ素を含む残り H202. 5 Sinustop ハーブ充血除去剤錠 60 mg 結晶塩酸プソイド エフェドリン HCl 各を含むいくつかのハーブ素材と混合されます。またはいくつかの他の方法を通じて得られたエフェドリンの 300 mg。3. 5 道路フレア。4. ドレイン クリーナー含有濃硫酸の瓶5. ボトルの白い蒸留酢6. 赤い悪魔苛性アルカリ溶液含む水酸化ナトリウム7. スプレーは、ブレーキ クリーナー 1,1,1 トリクロロ エチレンまたは 1,1,1 トリクロロエタンを含む手順:A. 純化プソイド エフェドリン:1. 5 充血除去剤のカプセルを取る、コーヒー フィルターで小さい漏斗にその内容を空に。フィルター、50 ml の冷たい水を注ぐし、小瓶の液体を収集します。2. 収集した液に苛性アルカリ溶液の 1/4 tsp を追加します。すぐに、エフェドリンの匂いを嗅ぐべきであります。3 別の小瓶に入れ、結果ソリューションとクリーナー ブレーキの 50 ml を追加、その後、蓋を閉めるし、積極的に振る。されるので、レイヤーを立ってみましょう。4. 七面鳥バスターを使用してブレーキ クリーナー下層瓶から吸い上げるし、小さなボウルに入れて。5. 酢 50 ml を加え、結果冷温を水の 1/2 インチのフライパンで弱火で加熱します。こうして水浴。ストーブ、炎が付いている接触がある場合、ブレーキ クリーナー蒸気は有毒なホスゲンになりますので、ガスを使用しないでください。代わりに低温ホット プレートや電気コンロを使用します。6. 熱ないより多くの液体が残るまで風呂の水でボウル。下部プソイド エフェドリン酢酸の強固な層になります。B. 赤いリンの準備中。1. 5 のフレアのキャップ オフ赤リンをこすり、後で使用するため保存します。フレアあたり約 0.1 g を取得する必要があります。C. は、ヨウ素/ハワイ ソリューションを準備します。1. Pour the entire bottle of the iodine tincture into a small ceramic bowl. Heat on the above type water bath until no more alcohol is left. Let cool, put in a small polyethylene jar, and add 0.1ml of the H2SO4 drain cleaner. Thats about 1/4inch of liquid in the end of an eye dropper. This converts the sodium iodide to HI. You now have a solution of iodine and HI. 2. Add the red phosphorus, and heat bottle in a water bath until the purple iodine color goes away.D. The reaction:1. Add the pseudoephedrine acetate to the solution of HI/I and phosphorus, and heat on a water bath for 24 hours.E: Extraction:1. Cool the reaction solution and add 1/2tsp of lye. Take the solution and perform steps A3-A6. 2. You will end up with methamphetamine acetate that you can scrape from the bowl.Congradulations! You have circumvented all of law enforcement and have greatly contributed to the end of the “drug war”. (or contributed to the outlaw of all flares, iodine tincture, vignegar, drain cleaners, and auto store chemicals and coffee filters as will happen in the next year)Best regards, Cousin Singe————FAQ fodder…If methamphetamine looks waxy or oily, it is probably contaminated with the HI salt of meth, an oily by-product of the red-phosphorous/HI reduction of ephedrine–the most prevalent method of clandestine manufacture.The HI salt is soluble in acetone, while the HCL salt is only very slightly soluble. The HI salt could be washed out, basified, and then precipitated with HCl gas to give methamphetmine HCL.When completely dry, methamphetamine HCL is soluble in chloroform, while ephedrine HCL is not. This would provide a convenient method of separation.[Reference: Skinner, Harry F., "Methamphetamine Synthesis Via Hydriotic Acid/Red Phosphorous Reduction Of Ephedrine," Forensic Science International, Vol 48, 1990, pp. 123-134]
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